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Chemistry
"A Manual for General Chemistry Laboratory
I, 2045L"
7th edition
James C. Horvath, University of Florida
ISBN: 0-89892-381-6
This manual is for the first lab course in
General Chemistry at the University of Florida. It has been in
publication for many years and was developed to make Chemistry
students "think" in the lab as opposed to filling in blanks. Dr.
Horvath believes that knowledge with understanding is much more
valuable than simple knowledge.
Table of
Contents
Foreward
Laboratory Instructions
ASSIGNMENTS
1- Measuring Mass(Weight) and Volume
2- Density
3- Classes of Matter- Changes in Matter- Chemical Formulas and
Equations
4- Stoichiometry
5- Stoichiometry of a Reaction in Solution- Introduction to
Bronsted-Lowry Acid-Base Chemicals
6- Solution Conductivity- Dissociation and Ionization- More on
Bronsted-Lowry Acid-Base Chemicals
7- Oxidation and Reduction (Redox)
8- Electrolytes and Nonelectrolytes- Still More on
Bronsted-Lowry Acid-Base Chemicals- Equilibrium
9- The Structure and Geometry of Molecules and Polyatomic Ions
10- Gases
11- Solutions
12- Chemical Kinetics
"Experiments in Organic
Chemistry"
3rd Edition
Richard K. Hill, emeritus University of Georgia
John Barbaro, Rocky Mountain College, formerly of University of
Florida
ISBN: 0-89892-311-5
Originally written for the University of
Georgia Organic Chemistry labs, this manual has been expanded and
now has over 50 adoptions throughout the country. Most of the lab
manual's experiments are small-scale, using 1-5 g of starting
materials, and a large majority are also designed for microscale
laboratories, using 50-200 mg of reagents, making this manual
suitable for both standard or microscale operations.
Table of
Contents
Prefece and Acknowledgments
GENERAL INFORMATION
G1- Safety and Waste Disposal
G2- Laboratory Notebook and Lab Reports
G3- Glassware
FUNDAMENTAL LABORATORY TECHNIQUES
T1- General techniques
T2- Recrystallization
T3- Melting Points
T4- Distillation
T5- Extraction
T6- Drying and Drying Agents
T7- Thin-layer Chromatography
T8- Gas Chromatography
T9- Calculation of Percent Yield
EXPERIMENTS
E1- Purification of an Unknown Solid by Recrystallization and
Identification by Melting Point
E2- Distillation
E3- Thin-layer Chromatography
E4- Extraction of Organic Compounds from Natural Sources
E5- Dehydration of Alcohols
E6- Preparation of Diphenylacetylene
E7- The Diels-Alder Reaction
E8- Preparation and Substitution Reactions of Alkyl Halides
E9- Electrophilic Aromatic Substitution: Nitration
E10- Friedel-Crafts Reactions
E11- Oxidation of Alcohols: Preparation of Camphor
E12- The Aldol Condensation: Preparation of Dibenzalacetone
E13- The Knoevenagel Condensation: Preparation of Ethel
3-Coumarincarboxylate
E14- Identification of an Unknown Aldehyde or Ketone
E15- The Wittig Reaction: Preparation of
1,4-Diphenyl-1,3-butadiene, and E-9-(2-Phenylethenyl)anthracene
E16- The Grignard Reaction: Preparation of Triphenylmethanol &
Benzoic Acid
E17- The Williamson Ether Synthesis: Preparation of an
Aryloxyacetic Acid from Cresol
E18- Fischer Esterification
E19- Preparation of Aspirin
E20- Amides
E21- Formation and Reactions of Cyclic Anhydrides
E22- Oxidative Coupling of 2-Naphthol
E23- Reactions of Aryl Diazonium Salts
E24- Carbohydrates
E25- Sodium Borohydride Reduction of Benzil and Determination of
Acetonide Stereochemistry by H NMR
E26- Hydrogenation of Olive Oil
MYSTERY REACTIONS
APPENDIX
"A Manual for General Chemistry
Laboratory II, 2046L"
3rd edition
James C. Horvath, University of Florida
ISBN: 0-89892-386-7
This manual is for the second lab course
in General Chemistry at the University of Florida. It has been in publication
for 20 years and espouses the same teaching philosophy as it's precursor.
Table of
Contents
Foreward
Laboratory Instructions
Acid/Base and Solubility Table
Table of Equilibrium Constants
ASSIGNMENTS
1- Acid/Base Strength-Equilibrium-pH-Indicators-Buffers
2- Introduction to Qualitative Analysis
3- Ca2+ and CO32-
4- Mg(OH2)62+ and Al(OH2)63+
5- Review of Ions- I
6- Zn(OH2)62+, Cu(OH2)62+,
and Ag(OH2)2+
7- Carbonates and Sulfides of Zn2+, Cu2+,
and Ag+
8- Sulfides in HONO2 (HNO3) Solution
9- Review of Ions- II
10- Fe(OH2)63+ and Cr(OH2)63+
11- Review of Ions- III
"Experiments in General Chemistry"
11th edition
Stephen H. Swann, Auburn University
ISBN: 0-89892-380-8
This manual was originally written in 1983 by W.D. Perry and has
been revised over the years to meet the requirements of a General
Chemistry laboratory.
Table of
Contents
Preface
Laboratory Policies
Excused Absence Request
Lab Reports
Check-in/ Check-out
Common Laboratory Equipment
EXPERIMENTS
1- Determination of Density
2- Determination of Avagadro's Number
3- Determination of the Formula of a Hydrate
4- Determination of the Composition of a Compound
5- Stoichiometric Ratio
6- The Gas Constant
7- Molecular Weight of a Volatile Compound
8- Determination of Reaction Stoichiometry
9- Determination of the Percent Acetic Acid in a Vinegar Sample
10- Molecular Weight Determination by Freezing Point Depression
11- Enthalpy of Hydration
12- Chemical Kinetics
13- Acid Dissociation Constant
14- Kinetics of a Chemical Reaction: Concentration Dependence of
the Reaction of Iodide w/ Persulfate
15- The Chemistry and Qualitative Analysis of Cations: Group 1
16- The Chemistry and Qualitative Analysis of Cations: Group 2
17- Buffer Solutions
18- Spectrophotometric Determination of Food Dyes
19- Preparation of Alum from Aluminum Metal
20- Determination of the Solubility Product: Mg(OH)2
21- Redox Titrations
22- Separating and Identifying Food Dyes by Paper Chromatography
APPENDIX
1- Errors and Significant Figures
2- Use of Glassware
Graph Paper
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