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Chemistry
"Experiments in General,
Organic,
and Biological Chemistry, Featuring MeasureNet" 4th edition
Bobby Stanton, University of Georgia
Lin Zhu, University of Georgia
ISBN: 0-89892-317-4, shrink-wrapped loose pages
University of Georgia authors Bobby Stanton and Lin
Zhu have revised their laboratory manual for
non-science majors. In the Fourth Edition, due March
2006, they have added extensive procedures using
MeasureNet’s integrated, networked data collection
system. The manual features innovative experiments,
as well as collaborative, multi-component chemical
analysis. Incorporating MeasureNet into the
laboratories affords students the opportunity to
collect and manipulate scientific data in a manner
comparable to that of their future employers. This
manual also contains self-directed experiments and can
be used without MeasureNet.
Table of Contents
Laboratory Safety Rules
Laboratory Equipment
EXPERIMENTS
1- Measurements
2- Physical and Chemical Changes
3- Specific Heat of a Metal
4- Empirical Formula of Magnesium Oxide
5- Formula of a Hydrate
6- Emission Analysis of Metals
7- Self Directed-Identity of an Unknown Metal
8- Types of Chemical Reactions
9- Recycling of Aluminum
10- Rates of Chemical Reactions
11- Chemical Equilibria
12- Determination of the Molecular Weight of a Volatile Liquid
Using the Ideal Gas Law
13- Concentration of Acetic Acid in Vinegar
14- Efficiency of Antacid Tablets
15- pH, Buffer Solutions, and the Henderson-Hasselbalch Equation
16- Paper Recycling and Aging
17- Self Directed-Quality Control for GlassEx
18- Hydrocarbons
19- Alcohols and Phenols
20- Aldehydes and Ketones
21- Carboxylic Acids and Esters
22- Amines and Amides
23- Self Directed- Identification of an Unknown Organic Compound
24- Carbohydrates
25- Amino Acids and Protiens
26- Titration of Vitamin C
27- Soaps and Detergents
28- Polymerization Reactions
29- Chromatography
30- Dyeing of Fabrics
31- Stoichiometry
Appendicies
"Experiments in Organic Chemistry" 3rd Edition
Richard K. Hill, emeritus University of Georgia
John Barbaro, Rocky Mountain College, formerly of University of
Florida
ISBN: 0-89892-311-5
Originally written for the University of Georgia
Organic Chemistry labs, this manual has been expanded and now has
over 50 adoptions throughout the country. Most of the lab manual's
experiments are small-scale, using 1-5 g of starting materials, and
a large majority are also designed for microscale laboratories,
using 50-200 mg of reagents, making this manual suitable for both
standard or microscale operations.
Table of Contents
Prefece and Acknowledgments
GENERAL INFORMATION
G1- Safety and Waste Disposal
G2- Laboratory Notebook and Lab Reports
G3- Glassware
FUNDAMENTAL LABORATORY TECHNIQUES
T1- General techniques
T2- Recrystallization
T3- Melting Points
T4- Distillation
T5- Extraction
T6- Drying and Drying Agents
T7- Thin-layer Chromatography
T8- Gas Chromatography
T9- Calculation of Percent Yield
EXPERIMENTS
E1- Purification of an Unknown Solid by Recrystallization and
Identification by Melting Point
E2- Distillation
E3- Thin-layer Chromatography
E4- Extraction of Organic Compounds from Natural Sources
E5- Dehydration of Alcohols
E6- Preparation of Diphenylacetylene
E7- The Diels-Alder Reaction
E8- Preparation and Substitution Reactions of Alkyl Halides
E9- Electrophilic Aromatic Substitution: Nitration
E10- Friedel-Crafts Reactions
E11- Oxidation of Alcohols: Preparation of Camphor
E12- The Aldol Condensation: Preparation of Dibenzalacetone
E13- The Knoevenagel Condensation: Preparation of Ethel
3-Coumarincarboxylate
E14- Identification of an Unknown Aldehyde or Ketone
E15- The Wittig Reaction: Preparation of
1,4-Diphenyl-1,3-butadiene, and E-9-(2-Phenylethenyl)anthracene
E16- The Grignard Reaction: Preparation of Triphenylmethanol & Benzoic Acid
E17- The Williamson Ether Synthesis: Preparation of an
Aryloxyacetic Acid from Cresol
E18- Fischer Esterification
E19- Preparation of Aspirin
E20- Amides
E21- Formation and Reactions of Cyclic Anhydrides
E22- Oxidative Coupling of 2-Naphthol
E23- Reactions of Aryl Diazonium Salts
E24- Carbohydrates
E25- Sodium Borohydride Reduction of Benzil and Determination of
Acetonide Stereochemistry by H NMR
E26- Hydrogenation of Olive Oil
MYSTERY REACTIONS
APPENDIX
"A Manual for General
Chemistry Laboratory I, 2045L" 5th edition
James C. Horvath, University of Florida
ISBN: 0-89892-215-1
This manual is for the first lab course in
General Chemistry at the University of Florida. It has been in
publication for many years and was developed to make Chemistry
students "think" in the lab as opposed to filling in blanks. Dr.
Horvath believes that knowledge with understanding is much more
valuable than simple knowledge.
Table of Contents
Foreward
Laboratory Instructions
ASSIGNMENTS
1- Measuring Mass(Weight) and Volume
2- Density
3- Classes of Matter- Changes in Matter- Chemical Formulas and
Equations
4- Stoichiometry
5- Stoichiometry of a Reaction in Solution- Introduction to
Bronsted-Lowry Acid-Base Chemicals
6- Solution Conductivity- Dissociation and Ionization- More on
Bronsted-Lowry Acid-Base Chemicals
7- Oxidation and Reduction (Redox)
8- Electrolytes and Nonelectrolytes- Still More on Bronsted-Lowry
Acid-Base Chemicals- Equilibrium
9- The Structure and Geometry of Molecules and Polyatomic Ions
10- Gases
11- Solutions
12- Chemical Kinetics
"A Manual for General
Chemistry Laboratory II, 2046L" 2nd edition
James C. Horvath, University of Florida
ISBN: 0-89892-147-3
This manual is for the second lab course in
General Chemistry at the University of Florida. It has been in
publication for 15 years and espouses the same teaching philosophy
as it's precursor.
Table of Contents
Foreward
Laboratory Instructions
Acid/Base and Solubility Table
Table of Equilibrium Constants
ASSIGNMENTS
1- Acid/Base Strength-Equilibrium-pH-Indicators-Buffers
2- Introduction to Qualitative Analysis
3- Ca2+ and CO32-
4- Mg(OH2)62+ and Al(OH2)63+
5- Review of Ions- I
6- Zn(OH2)62+, Cu(OH2)62+,
and Ag(OH2)2+
7- Carbonates and Sulfides of Zn2+, Cu2+,
and Ag+
8- Sulfides in HONO2 (HNO3) Solution
9- Review of Ions- II
10- Fe(OH2)63+ and Cr(OH2)63+
11- Review of Ions- III
"Experiments in General
Chemistry" 9th edition
Stephen H. Swann, Auburn University
ISBN: 0-89892-344-1
This manual was originally written in 1983 by W.D.
Perry and has been revised over the years to meet the requirements
of a General Chemistry laboratory.
Table of Contents
Preface
Laboratory Policies
Excused Absence Request
Lab Reports
Check-in/ Check-out
Common Laboratory Equipment
EXPERIMENTS
1- Determination of Density
2- Determination of Avagadro's Number
3- Determination of the Formula of a Hydrate
4- Determination of the Composition of a Compound
5- Stoichiometric Ratio
6- The Gas Constant
7- Molecular Weight of a Volatile Compound
8- Determination of Reaction Stoichiometry
9- Determination of the Percent Acetic Acid in a Vinegar Sample
10- Molecular Weight Determination by Freezing Point Depression
11- Enthalpy of Hydration
12- Chemical Kinetics
13- Acid Dissociation Constant
14- Kinetics of a Chemical Reaction: Concentration Dependence of
the Reaction of Iodide w/ Persulfate
15- The Chemistry and Qualitative Analysis of Cations: Group 1
16- The Chemistry and Qualitative Analysis of Cations: Group 2
17- Buffer Solutions
18- Spectrophotometric Determination of Food Dyes
19- Preparation of Alum from Aluminum Metal
20- Determination of the Solubility Product: Mg(OH)2
21- Redox Titrations
22- Separating and Identifying Food Dyes by Paper Chromatography
APPENDIX
1- Errors and Significant Figures
2- Use of Glassware
Graph Paper
"LABTREK: Experiments for
General Chemistry"
3rd edition
Jay H. Worrell, University of South Florida
ISBN: 0-89892-154-6
A general Chemistry lab manual that is suitable
for both large and small Chemistry programs. It builds on skills and
information learned in the early experiments dealing with
nomenclature, writing compound formulas, using chemical names and
writing balanced chemical reactions.
Table of Contents
Preface
Laboratory Check-In
EXPERIMENTS
1- Data Analyses: Precision, Uncertainty, Significant Figures,
and Error
2- Physical Properties of Compounds: Density, Melting Point, and
Boiling Point
3- Using Basic Laboratory Operations to Separate the Components
of a Mixture
4- Separation of a Mixture Into Pure Components, Paper
Chromatography
5- The Language of Chemistry: Chemical Formulas, Nomenclature,
and Chemical Reactions
6- The Determination of Avagadro's Number
7- Compound Composition and Water of Hydration
8- Classification of Chemical Reactions and Mass-to-Mole
Calculations
9- Balancing Chemical Reactions, Stoichiometry and Mole-Mass
Relationships
10- Determination of a Compound's Formula
11- Properties and Tests for Several Commonplace Ions that are
Basic Building Blocks for Numerous Compounds
12- The Preparation and Properties of Covalent Molecular
Compounds
13- Molecular Mass Determination for a Low-Boiling Liquid
14- Determination of Absolute Zero Using Charles' Law: The
Temporature-Volume Dependence for Gases
15- Product Analysis and Balancing Oxidation-Reduction Reactions
16- Oxidaiton-Reduction Titration Reactions
17- Heat, Enthalpy, and Chemical Reactions: The Heat of
Neutralization
18- Heat, Enthalpy, and Chemical Reactions: The Heat of Solution
and Hess's Law
19- Physical and Chemical Properties of the Alkaline Earth and
Halogen Elements
20- Qualitative Analysis for Ag(I), Pb(II), and Hg2(II)
Cations
21- The System: An Exercise in Observation and Deductive
Reasoning Skills, the Scientific Method
22- Substitution Reactions at a Copper(II) Center
23- Attractive Forces Between Molecules and Ions and the
Physical Properties of Materials
24- Application of a Colligative Property: Determination of the
Formula Mass for a Soluble Solute
25- The Preparation, Isolation, and Characterization of Aspirin
26- An Inorganic Synthesis: The Reaction Between Tin and Iodine
27- Qualitative Analysis for a Mixture of Mg(II), Ca(II), Ba(II),
Mn(II), Fe(III), Co(II), Ni(II), Cu(II) and Al(III) Cations
28- Qualitative Analysis for Cu(II), Bi(III), Sn(IV), and Sb(III)
Cations
29- The Separation and Qualitative Identification of Several
Transition Metal Ions
30- Quantitative Anaysis Using a Spectronic-20 and the
Beer-Lambert Law
31- Systems in Equilibrium; Applications of Le Chatelier's
Principle
32- Systems in Equilibrium; The Determination of Equilibrium
Constants
33- The Titration of Acids and Bases, Quantitative Chemistry
34- Acids and Bases and the Measurement of pH
35- Voltaic Cell Measurements
36- Kinetics and Mechanism of a Chemical Reaction
37- Spectroscopy: The Study of Electronic Transitions
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